Photochemical and Beckmann rearrangement of (Z)-cholest-4-en-6-one oxime

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Photochemical Rearrangement of 8- methyl Spiro [2.5] oct-7-en-4-one to 4-methyl Spiro [2.5] oct-4-en-6-one

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photochemical rearrangement of 8- methyl spiro [2.5] oct-7-en-4-one to 4-methyl spiro [2.5] oct-4-en-6-one

irradiation of &methyl; spiro [2.5] oct-7-en-4-one through its singlet excited state resulted in the formation of 4-methyl spiro [2.5] oct-4-en -6-one. we have used the cyclopropyl moiety in the molecule as a probe to study the operating mechanism in the photochemistry of ?, ?-unsaturated compounds. the results showed that this photoisomerization probably occurs through a concerted process.

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Identification and Characterization of TRO19622 (Cholest-4-en-3- One, Oxime), a Novel Drug Candidate for Amyotrophic Lateral Sclerosis

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Cholest-5-en-7-one

In the deca-hydro-phenanthrenone ring system of the title compound, C(27)H(44)O, the two cyclo-hexane rings adopt chair conformations, whereas the cyclo-hexene ring adopts an envelope conformation. The cyclo-pentane ring is twisted. In the crystal structure, mol-ecules are stacked along the a axis, but no significant inter-molecular inter-actions are observed.

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ژورنال

عنوان ژورنال: Journal of the Serbian Chemical Society

سال: 2004

ISSN: 0352-5139,1820-7421

DOI: 10.2298/jsc0406413k